Determinants (Mathematical Monographs No. 3), Fourth by Laenas Gifford Weld

By Laenas Gifford Weld

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Another possibility is the use of a two step process. In the first step, PET is hydrolysed for 30min at 220°C to 280°C in a twin extruder. The partly hydrolysed slurry is cooled and the precipitated solid is separated from the mother liquid. The solid is dissolved in an ammonia solution after that, and the hydrolysis is finished at 180°C to 230°C after 30min reaction. TPA is precipitated by adding sulfuric acid [53]. The most processes described above are also under consideration as industrial relevant processes.

Korea. , Korea. According to the supplier, their length and diameter were in the range of 10-50 μm and 10-30 nm, respectively, indicating that their aspect ratio reached 1000. All materials were dried at 120 °C in vacuo for at least 24 h before use, to minimize the effects of moisture. The PEN/CNT nanocomposites were prepared by a melt blending process in a Haake rheometer (Haake Technik GmbH, Germany) equipped with a twin-screw (nonintermeshing co-rotating type). The temperature of the heating zone, from the hopper to the die was set to 280, 290, 295, and 285 oC, and the screw speed was fixed at 20 rpm.

Korea. According to the supplier, their length and diameter were in the range of 10-50 μm and 10-30 nm, respectively, indicating that their aspect ratio reached 1000. All materials were dried at 120 °C in vacuo for at least 24 h before use, to minimize the effects of moisture. The PEN/CNT nanocomposites were prepared by a melt blending process in a Haake rheometer (Haake Technik GmbH, Germany) equipped with a twin-screw (nonintermeshing co-rotating type). The temperature of the heating zone, from the hopper to the die was set to 280, 290, 295, and 285 oC, and the screw speed was fixed at 20 rpm.

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